C.A.T. GmbH & Co. Chromatographie und Analysentechnik KG

Heerweg 10
D-72070 Tübingen
Germany

Phone: +49 (0) 7071 / 78323
Fax: +49 (0) 7071 / 75163

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Sample amounts

Unbenanntes Dokument

We need the following sample amounts plus some additional amount for sample handling.

AAA    Enantiomerlabeling

At least 3mg, better 5mg

without determination of blind values

At least 1mg, better 3mg

other amino acids

At least 2mg, better 5mg

AcOH / TFA – content

At least 3mg, better 5mg

Enantiomeric purity of amino acid derivatives

At least 2mg, better 5mg

Enantiomeric purity of peptides (GC-MS)

At least 1mg, better 5mg
(depends on the length of peptide)

Residuals of solvents

At least 3mg, better 5mg

 

 

For analyses in duplicate the required sample amount is double.

The amount needed for sample handling depends on the physical properties. A freeze dried product needs nearly no additional amount whereas an oily product some 10mg’s.

These amounts are necessary to obtain the required accuracy of the weighing process (minimum weight in accordance to USP) and the required LOQ’s.

Please ask if these sample amounts are not available.

Last Updated (Thursday, 02 September 2010)